[1]杨 蓉,丁建宁,丁古巧,等.高纯铝片抛光工艺及对氧化铝模板的影响[J].常州大学学报(自然科学版),2011,(02):6-10.
　YANG Rong,DING Jian-ning,DING Gu-qiao,et al.Study of Electrochemical Polishing on Al and the Influence on Porous Anodic Alumina[J].Journal of Changzhou University(Natural Science Edition),2011,(02):6-10.
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高纯铝片抛光工艺及对氧化铝模板的影响()
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常州大学学报(自然科学版)[ISSN:2095-0411/CN:32-1822/N]

卷:
期数:
2011年02期
页码:
6-10
栏目:
材料科学与工程
出版日期:
2011-03-30

文章信息/Info

Title:
Study of Electrochemical Polishing on Al and the Influence on Porous Anodic Alumina
作者:
杨 蓉1; 丁建宁1; 2; 丁古巧1; 袁宁一1; 2
1.常州大学 低维材料微纳器件与系统研究中心,江苏 常州 213164; 2.江苏省新能源材料与技术重点实验室,江苏 常州 213164
Author(s):
YANG Rong1; DING Jian-ning1; 2; DING Gu-qiao1; YUAN Ning-yi1; 2
1.Center for Low-Dimensional Materials,Micro-Nano Devices and System,ChangzhouUniversity,Changzhou 213164,China; 2.Jiangsu Key Laboratory for Solar Cell Materials and Technology, Changzhou 213164, China
关键词:
电化学抛光;  多孔阳极氧化铝模板;  表面平整度
Keywords:
electrochemical polishing;  porous anodic alumina;  flatness
分类号:
TQ 586.5
文献标志码:
A
摘要:
在多孔阳极氧化铝(Porous anodic alumina, PAA)制备过程中,为了得到更稳定的电解过程,实现高度有序的纳米孔阵列结构,对高纯铝片表面进行抛光是一个典型的、必要的步骤。为此系统研究了高氯酸/乙醇抛光液体系在不同电压(1,5,10,20 V和25 V)和不同时间(10,60 s和180 s)下的抛光工艺,以及抛光对高纯铝片表面以及PAA的影响,获得用于制备PAA模板较合适的抛光工艺,即抛光电压为10V,抛光时间为180 s。
Abstract:
During the preparation of Porous anodic alumina(PAA), toget a stable electrolysis and an ordered nano-size polar arrangement, the electrochemical polishing is usually required. However, there have been few systematic and detailed studies on the influence of polishing on the Al film flatness, the growth and order degree of PAA. In this paper different voltage(1, 5, 10, 20 V and 25 V)and different polishing time(10, 60 s and 180 s)in the mixture of perchloric acid(60%)and ethanol were chosen to study the effect of polish on surface of Al and the growth of PAA. The study indicates that the optimum technical parameters are as follows: polishing voltage of10 V and polishing time of 180 s.

参考文献/References:

[1]Masuda H,Fukuda K. Ordered metal nanohole arrays made by a two-step replication of honeycomb structures of anodic alumina[J]. Science, 1995, 268: 1466-1 468.
[2]Masuda H,Yada K,Osaka A. Self-ordering of cell con?guration of anodic porous alumina with large-size pores in phosphoric acid solution[J]. Japanese Journal of Applied Physics, 1998, 37: L1 340-L1 342.
[3]Nielsch K,Choi J,Schwirn K.Self-ordering regimes of porous alumina: The 10% porosity rule[J]. Nano Letters, 2002, 2: 677-680.
[4]Li A P,Müller F,G(¨overo)sele U. Pore and monocrystalline pore arrays withlarge interpore distance in anodic alumina[J]. Electrochemical and Solid-StateLetters, 2000, 3(3): 131-134.
[5]Zhang W M,Qian J Q,Huang Z P. Experiment and research on development and characterizations of anodic alumina membrance for use in homodialysis[J]. Journal of Shanghai Second Medical University, 2005, 17(1): 38-42.
[6]Zhao S Y,Chan K R,Yelon A. Novel structure of AAO film fabricated by constant current anodization[J]. Advanced Materials,2007, 19: 3 004-3 007.
[7]Mei Y F,Huang G S,Li Z M,et al. Formation of Si-based nano-island array on porous anodic alumina[J]. Acta Materialia, 2004, 52: 5 633-5 637.
[8]Jung M,Kimb H G,Lee J K,et al. EDLC characteristics of CNTs grown on nanoporous alumina templates[J]. Electrochimica Acta,2004, 50: 857-862.
[9]Bocchetta P,Sunseri C,Chiavarotti G,et al. Microporous alumina membranes electrochemically grown[J]. Electrochimica Acta, 2003, 48: 3 175-3 183.
[10]Li Y,Ling Z Y,Chen S S,et al. Fabrication of novel porous anodic aluminamembranes by two-step hard anodization[J]. Nanotechnology, 2008, 19: 225604.
[11]Jha H,Kikuchi T,Sakairi M,et al. Synthesis of aluminum oxy-hydroxide nanofibers from porous anodic alumina[J]. Nanotechnology,2008,19:395603.

备注/Memo

备注/Memo:
基金项目:常州市科技支撑项目资助(CE20100047) 作者简介:杨蓉(1986-),女,江苏大丰人,硕士生; 通讯联系人:丁建宁。
更新日期/Last Update: 2011-03-30