[1]郭登峰,金凤明.气相色谱法分析二乙二醇甲醚[J].常州大学学报(自然科学版),2000,(04):32-34.
 GUO Deng -feng,JIN Feng -ming.Determination of Diethyleneglycol Monomethy l Ether by Gas Chromatography[J].Journal of Changzhou University(Natural Science Edition),2000,(04):32-34.
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气相色谱法分析二乙二醇甲醚()
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常州大学学报(自然科学版)[ISSN:2095-0411/CN:32-1822/N]

卷:
期数:
2000年04期
页码:
32-34
栏目:
出版日期:
2000-12-25

文章信息/Info

Title:
Determination of Diethyleneglycol Monomethy l Ether by Gas Chromatography
作者:
郭登峰 金凤明
江苏石油化工学院化学工程系, 江苏 常州 213016
Author(s):
GUO Deng -feng JIN Feng -ming
Department of Chemical Engineering , Jiangsu Institute of Pet rochemical Technology , Chang zhou 213016 , China
关键词:
二乙二醇甲醚气相色谱法分解
Keywords:
diethy leneg ly col monomethy l ether gas chromatog raphy analy sis
分类号:
O 658/ R 29
文献标志码:
A
摘要:
以GDX-103 色谱填充柱分离, 二乙二醇乙醚为内标物, 气相色谱法测定二乙二醇甲醚含量, 该法快速、准确、重现性 好。回收率在97.6 %~ 99.4 %, 相对标准偏差为0.17 %。
Abstract:
The contents of diethyleneglycol monomethyl ether were determined with gas chromatog raphy by using stainless steel column (2 m ×3 mm i.d.)packed wi th GDX -103 .The quantitative determination was perfo rmed with carbitol as the internal standard .The method was simple and rapid .The average recovery of diethyleneglycol monomethyl ether w as (97.6 ~ 99.4)%.The result showed good linearity (r =0.996 9)and relative standard deviation was 0.17 %.

参考文献/References:

[1] GB 10830 -1998, 机动车制动液使用技术条件[S] .
[2] 李浩春.分析化学手册(第五分册) [M] .北京:化学工业 出版社, 1999.260 -261.

相似文献/References:

[1]郭登峰,潘剑波,杨建男,等.衍生气相色谱法分析二丁基二氯化锡[J].常州大学学报(自然科学版),2000,(02):21.
 GUO Deng -feng,PAN Jian -bo,YANG Jian -nan,et al.Der ivative Gas Chromatographic Analysis of Bu2SnCl2[J].Journal of Changzhou University(Natural Science Edition),2000,(04):21.

备注/Memo

备注/Memo:
作者简介:郭登峰(1964 -), 男, 江苏南通人, 工程师, 主要从事化学分析方面的教学和研究。
更新日期/Last Update: 2000-12-25