[1]陈 烨,纪俊玲,李海乐,等.3- ( 三甲氧基硅烷基) 丙基二甲基十二烷基氯化铵 的合成及其抗菌性能[J].常州大学学报(自然科学版),2010,(02):10-14.
　CH EN Ye,JI Jun- ling,LI Hai- le,et al.Synthesis and Antibacterial Property of 3- ( Trimethoxysilyl) Propyldimethyldodecyl Ammonium Chloride[J].Journal of Changzhou University(Natural Science Edition),2010,(02):10-14.
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3- ( 三甲氧基硅烷基) 丙基二甲基十二烷基氯化铵 的合成及其抗菌性能()
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常州大学学报(自然科学版)[ISSN:2095-0411/CN:32-1822/N]

卷:
期数:
2010年02期
页码:
10-14
栏目:
出版日期:
2010-06-25

文章信息/Info

Title:
Synthesis and Antibacterial Property of 3- ( Trimethoxysilyl) Propyldimethyldodecyl Ammonium Chloride
作者:
陈 烨1 ; 纪俊玲1 ;  李海乐1;  葛海华2
1.常州大学化学化工学院, 江苏 常州 213164; 2.杭州奥坦斯布艺有限公司, 浙江 杭州 311100
Author(s):
CH EN Ye1 ;  JI Jun- ling1 ;  LI Hai- le1 ;  GE Hai- hua2
1. School of Chemical and Chemist ry Engineering, Changzhou Univer sity, Changzhou 213164, China; 2. Hangzhou Hig htex Co. , Ltd. , Hangzho u 311100, China
关键词:
阳离子;  季铵盐;  抗菌剂;  耐久
Keywords:
cationic surfactant;  quaternary ammonium salts;  ant ibacter ial finishing agent;  durability
分类号:
T Q 264
文献标志码:
A
摘要:
以C- 氯丙基三甲氧基硅烷、十二烷基二甲基叔胺为原料, 碘化钠为催化剂合成有机硅季铵盐抗菌剂, 考察了溶剂、催 化剂用量、反应时间等因素对季铵化反应的影响。实验结果表明, 以甲醇、二甲亚砜作混合溶剂, 溶剂用量30%, 碘化钠相对 摩尔用量01 05, 反应温度65 e , 反应48 h 后的反应收率可达821 39%。同时考察了在不同整理工艺条件下用有机硅季铵盐整 理不同织物后各织物的抗菌效果, 为工业化生产及后整理提供方法和依据。
Abstract:
A ty pe o f silico ne quater nary ammonium salt w as sy nthesized by quaterisat ion react io n w ith 3- chloro pro py ltr imethox ysilane and N, N - Dimethy ldodecylamine, and the catalyzer w as sodium iodide. Some factors had been studied for the synthesis, such as the so lvent , the dosage o f sodium iodide and the react io n time. From these ex periment s, the optimal react ion co ndit ions w ere found in mix ing the same amount of the tw o raw materials in the admix ture so lvent of methanol and dimethyl sulfox ide at 65 e for 48 h. The comparative dosag e o f cataly zer used in this act ion w as 01 05. And the y ield of the product w as 821 39%. Some ant ibacter ial test s had also been do ne on dif ferent fabr ics w ith dif ferent techniques. These tests w ere suitable for indust rialized product io n and after- f inishing.

相似文献/References:

[1]裘兆蓉,裴峻峰,花震言,等.阳离子高分子絮凝剂F2 合成及表征[J].常州大学学报(自然科学版),2003,(01):17.
　Q IU Zhao -rong,PEI Jun -feng,HUA Zhen -yan,et al.Synthesis and Character istics of Cation Polymeric Flocculant F2[J].Journal of Changzhou University(Natural Science Edition),2003,(02):17.

备注/Memo

备注/Memo:
基金项目: 常州大学科技基金项目( 09020012) 作者简介: 陈烨( 1985- ) , 女, 江苏常熟人, 硕士研究生; 通讯联系人: 纪俊玲。
更新日期/Last Update: 2010-06-25